doi:10.16178/j.issn.0528-9017.20212854

Abstract

CLC Number:

S634
O657.63

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References 7

[1]	许晓敏, 李凌云, 林桓, 等. 基质效应对液相色谱串联质谱分析农药残留的影响研究[J]. 农产品质量与安全, 2019,(6):11-15,20.
[2]	吴淑春, 程珊莉, 梁赤周, 等. 普通白菜作为替代基质解决液相色谱-串联质谱基质效应的可能性[J]. 浙江农业科学, 2019, 60(5):819-822.
[3]	BASILICATA P, MIRAGLIA N, PIERI M, et al. Application of the standard addition approach for the quantification of urinary benzene[J]. Journal of Chromatography B, 2005, 818(2):293-299. DOI URL
[4]	YARITA T, AOYAGI Y, OTAKE T. Evaluation of the impact of matrix effect on quantification of pesticides in foods by gas chromatography-mass spectrometry using isotope-labeled internal standards[J]. Journal of Chromatography A, 2015, 1396:109-116. DOI URL
[5]	RIMAYI C, ODUSANYA D, MTUNZI F, et al. Alternative calibration techniques for counteracting the matrix effects in GC-MS-SPE pesticide residue analysis-A statistical approach[J]. Chemosphere, 2015, 118:35-43. DOI URL
[6]	许秀丽, 赵海香, 李礼, 等. 分析保护剂补偿基质效应-气相色谱-质谱法快速测定水果中40种农药残留[J]. 色谱, 2012, 30(3):267-272.
[7]	STAHNKE H, KITTLAUS S, KEMPE G, et al. Reduction of matrix effects in liquid chromatography-electrospray ionization-mass spectrometry by dilution of the sample extracts: how much dilution is needed?[J]. Analytical Chemistry, 2012, 84(3):1474-1482. DOI URL

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分析物	离子对	保留时间/min	碰撞能量/eV	分析物	离子对	保留时间/min	碰撞能量/eV
甲胺磷	141-95^*,141-80	4.318	5,20	甲基异柳磷	199-121^*,198.9-166.7,240.8-198.9	10.252	10,5,5
敌敌畏	109-79^*,184.9-93	4.617	10,5	喹硫磷	192.9-129^*,192.9-101.9,146-118	10.087	10,30,10
乙酰甲胺磷	136-42^*,136-94	5.582	15,5	腐霉利	283-96^*,282.8-68.0,284.8-96.0	10.688	10,25,10
氧乐果	156-110,110-79^*	6.660	10,15	丙溴磷	207.9-63^*,338.8-268.7	11.379	30,20
α-666	216.9-181^*,218.9-183	7.526	5,5	虫螨腈	137-102^*,247.1-227.1	11.885	15,5
乐果	86.9-46^*,142.9-111	7.675	10,15	三唑磷	257-162^*,285-257	12.485	15,5
β-666	216.9-181.1^*,181-145	7.937	5,15	异菌脲	313.8-55.9^*,313.8-244.9	13.537	20,10
γ-666	216.9-181.1^*,181-145	8.026	5,15	亚胺硫磷	160-77.1^*,160-133,160-105	13.730	20,20,15
δ-666	217-181.1^*,181.1-145.1	8.404	5,15	联苯菊酯	181.2-165.2^*,181.2-166.2	13.736	25,10
五氯硝基苯	295-237^*,236.9-142.9	8.099	20,30	甲氰菊酯	181.1-152.1^*,207.9-181	13.862	25,5
二嗪磷	137.1-84^*,137.1-54	8.156	10,20	伏杀硫磷	182-111^*,121.1-65	14.403	15,10
百菌清	263.8-133^*, 263.8-229,263.8-168	8.469	20,25,40	氯氟氰菊酯	181.1-152.1^*;208.1-181.1	14.616	30,10
乙烯菌核利	187-124^*,197.9-145	8.975	15,20	氯菊酯	183.1-168.1^*;183.1-153.1	15.501	10,15
甲基对硫磷	125-47^*,263.2-109	9.004	10,10	氟氯氰菊酯	162.9-127.0^*;162.9-90.9	16.105	10,10
杀螟硫磷	277-260^*,277-125	9.445	5,20	氯氰菊酯	163.0-127;181.0-152.0^*	16.409	25,10
马拉硫磷	172.9-99^*,173-127	9.587	5,15	氟氰戊菊酯	156.9-107.1^*,198.9-157	16.594	10,15
倍硫磷	124.9-79^*,124.9-47	9.292	5,10	氰戊菊酯	167-125.1^*,224.9-119	17.310	5,15
毒死蜱	198.9-171^*,314-258	9.805	12,15	氟胺氰菊酯	250.0-55.0^*,250.0-200.0	17.416	20,20
对硫磷	138.9-109^*,291-109	9.823	5,5	溴氰菊酯	181-152.1^*,250.7-172	17.820	25,5
三唑酮	208-127^*,208-181	9.863	20,5	4,4-滴滴滴	234.9-165.1^*,234.9-199.1,236.9-165.2	12.104	20,15,20
三氯杀螨醇	139-111^*,249.8-214.7,249.8-138.7	9.885	10,5,20	2,4-滴滴涕	235.0-165.2^*,235-199.1,237-165.2	12.160	20,15,20
水胺硫磷	135.9-108^*,135.9-69,121.0-65.1	9.931	15,30,15	4,4-滴滴伊	246.1-176.2^*,315.8-246.0,317.8-246.0	11.351	30,15,15
二甲戊灵	252.1-162.2^*,252.1-191	10.369	8.980	4,4-滴滴涕	235.0-165.2^*,235-199.2,237-165.2	12.755	20,15,20

分析物	离子对	保留时间/min	碰撞能量/eV	分析物	离子对	保留时间/min	碰撞能量/eV
甲胺磷	141-95^*,141-80	4.318	5,20	甲基异柳磷	199-121^*,198.9-166.7,240.8-198.9	10.252	10,5,5
敌敌畏	109-79^*,184.9-93	4.617	10,5	喹硫磷	192.9-129^*,192.9-101.9,146-118	10.087	10,30,10
乙酰甲胺磷	136-42^*,136-94	5.582	15,5	腐霉利	283-96^*,282.8-68.0,284.8-96.0	10.688	10,25,10
氧乐果	156-110,110-79^*	6.660	10,15	丙溴磷	207.9-63^*,338.8-268.7	11.379	30,20
α-666	216.9-181^*,218.9-183	7.526	5,5	虫螨腈	137-102^*,247.1-227.1	11.885	15,5
乐果	86.9-46^*,142.9-111	7.675	10,15	三唑磷	257-162^*,285-257	12.485	15,5
β-666	216.9-181.1^*,181-145	7.937	5,15	异菌脲	313.8-55.9^*,313.8-244.9	13.537	20,10
γ-666	216.9-181.1^*,181-145	8.026	5,15	亚胺硫磷	160-77.1^*,160-133,160-105	13.730	20,20,15
δ-666	217-181.1^*,181.1-145.1	8.404	5,15	联苯菊酯	181.2-165.2^*,181.2-166.2	13.736	25,10
五氯硝基苯	295-237^*,236.9-142.9	8.099	20,30	甲氰菊酯	181.1-152.1^*,207.9-181	13.862	25,5
二嗪磷	137.1-84^*,137.1-54	8.156	10,20	伏杀硫磷	182-111^*,121.1-65	14.403	15,10
百菌清	263.8-133^*, 263.8-229,263.8-168	8.469	20,25,40	氯氟氰菊酯	181.1-152.1^*;208.1-181.1	14.616	30,10
乙烯菌核利	187-124^*,197.9-145	8.975	15,20	氯菊酯	183.1-168.1^*;183.1-153.1	15.501	10,15
甲基对硫磷	125-47^*,263.2-109	9.004	10,10	氟氯氰菊酯	162.9-127.0^*;162.9-90.9	16.105	10,10
杀螟硫磷	277-260^*,277-125	9.445	5,20	氯氰菊酯	163.0-127;181.0-152.0^*	16.409	25,10
马拉硫磷	172.9-99^*,173-127	9.587	5,15	氟氰戊菊酯	156.9-107.1^*,198.9-157	16.594	10,15
倍硫磷	124.9-79^*,124.9-47	9.292	5,10	氰戊菊酯	167-125.1^*,224.9-119	17.310	5,15
毒死蜱	198.9-171^*,314-258	9.805	12,15	氟胺氰菊酯	250.0-55.0^*,250.0-200.0	17.416	20,20
对硫磷	138.9-109^*,291-109	9.823	5,5	溴氰菊酯	181-152.1^*,250.7-172	17.820	25,5
三唑酮	208-127^*,208-181	9.863	20,5	4,4-滴滴滴	234.9-165.1^*,234.9-199.1,236.9-165.2	12.104	20,15,20
三氯杀螨醇	139-111^*,249.8-214.7,249.8-138.7	9.885	10,5,20	2,4-滴滴涕	235.0-165.2^*,235-199.1,237-165.2	12.160	20,15,20
水胺硫磷	135.9-108^*,135.9-69,121.0-65.1	9.931	15,30,15	4,4-滴滴伊	246.1-176.2^*,315.8-246.0,317.8-246.0	11.351	30,15,15
二甲戊灵	252.1-162.2^*,252.1-191	10.369	8.980	4,4-滴滴涕	235.0-165.2^*,235-199.2,237-165.2	12.755	20,15,20

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